Isothermal Semi Batch Reactor

A isothermal semibatch reactor is a semiclosed system with one input stream It is operated under conditions like Isothermal Temperature of Reaction Mass remains constant and perfectly mixed composition of reaction mixture is uniform throughout This setup is used to study a noncatalytic homogeneous reaction under isothermal conditionThe set up consists of a Reactor fitted in a constant temperature water bath Before starting the reaction the reactor is charged with measured quantity of one reactant From a feed tank another reactant is fed to the reactor Using a sampling pipette samples can be taken out for analysis after fixed interval  One stirrer is fitted for mixing the reactants in reactor and other is fitted in water bath to keep the uniform temperature throughout in the bath The temperature of bath can be maintained from ambient to 70C with the help of Digital Temperature indicator Cum Controller.

Technical Specification :-

Reactor

Material Stainless Steel, Capacity 2 Ltrs (approx)

Water Bath

Material Stainless Steel, Double wall, insulated with Ceramic Wool

Heater

Nichrome wire Heater

Stirrer(2Nos.)

Stainless Steel Impeller and shaft coupled with FHP motor. (One each for Water Bath and Reactor)

Feed Tank (1Nos.)

Material Stainless Steel (1 Nos.), Capacity 20 Ltrs. with level indicators, air release valves, charging funnel with valve, air pressure fittings, feed lines, drain valve etc.

Feed Circulation

By Compressed Air, using PU pipe line & fittings Pressure Regulator Bourdon type (0-2 kg/cm2)

Flow Measurement

Rotameter

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