Packed Bed Distillation Column Apparatus
The column is made of Stainless Steel material packed with Borosilicate Glass rasching rings. An electrically heated reboiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form at the top of column are condensed in the shell and tube type condenser by circulating cooling water, supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation is provided for pressure & temperature measurement wherever necessary
Technical Specification :-
• Distillation Column : Material Stainless Steel , Dia. 80mm, Height 900mm (approx.)
• Packing Material : Borosilicate Glass Rasching Rings.
• Pressure Gauge : Bourdon type
• Rotameter : For cooling water flow rate measurement.
• Steam Generator : Made of Stainless Steel, provided with Pressure Gauge & Level Indicator, Safety valve & insulated with ceramic wool and cladding with Aluminium foil.
• Reflux Divider : Arrangement to change R/D ratio automatically.
• Condenser : Material Stainless Steel, Shell & Tube type
• Bottom Product Tank : Material Stainless Steel capacity 5 Ltrs.
• Distillate tank : Material Stainless Steel, capacity 5 Ltrs.
• Heaters : Nichrome wire heater.
• Temp. Sensors : RTD PT-100 type
• Control panel comprises of : Digital Temp. Controller : PID Controller, 0-199.9°C, (For Re-boiler) Digital Temp. Indicator : 0-199.9°C, with multi-channel switch Reflux timer : For changing R/D ratio With Standard make on/off switch, Mains Indicator etc.
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